Description

General description

The JEOL JEM-ARM300F2 (GrandARM) is a 300 kV double aberration-corrected transmission electron microscope (AC-TEM) with up to 53 pm imaging resolution in both STEM and TEM modes with X-ray energy dispersive spectroscopy (XEDS), electron energy loss spectroscopy (EELS), and segmented and 4D-STEM detectors for electric and magnetic field mapping. The GrandARM can be used to analyse a wide range of materials with imaging and spectroscopy at the atomic level, including nanoparticles and thin films and can utilise our range of in-situ holders for dynamic experiments.

Hardware specifications

Electron Optics

  • Electron Gun: cold field emission electron source
  • Acceleration voltage: 300 kV, 80 kV, 60 kV
  • Pole Piece: FHP2
  • Chromatic Aberration, Cc: 1.6 mm
  • Spherical Aberration, Cs: 0.7 mm
  • Image and Probe Cs Correctors: JEOL Eta Dodecapole Cs Corrector
  • Linear Information limit: 90 pm
  • STEM Resolution: 53 pm (300kV), 96 pm (80, 60 kV)

Cameras and Detectors

  • Gatan OneView (4kx4k; 25 fps).
  • Gatan NR post spectrometer Camera with Low Voltage Scintillator (2kx2k; 20 fps)
  • Gatan K3 post spectrometer Direct Electron Detector (3.4x3.4k; 70 fps)
  • Gatan Digiscan 3 (Model: 888) with STEMx
  • Gatan STEM detectors: Bright field, annular dark field
  • JEOL STEM detectors: Bright field, Annular dark field, Secondary and Back-scattered electron detectors, JEOL SAAF Segmented STEM Detector
  • Dual 158mm2 JEOL X-ray Energy Dispersive Spectrometers (XEDS) with a total collection area of 1.4 steradian
  • Gatan Continuum K3 (model 1069) Electron Energy Loss Spectrometer (EELS)

Sample Holders

  • JEOL Low Background Double Tilt Holders
  • JEOL Single Tilt Holders
  • JEOL High Tilt Holders (±70°) 
  • JEOL Liquid Nitrogen Cooling Holder 
  • Hummingbird 9 contact Heating and Biasing 
  • Hummingbird Liquid Flow cell 
  • Hummingbird Gas heating holder
  • Proto chips Atmosphere in-situ holder 
  • Simple Origin cryo-transfer holder 
  • Fischione Gas/Vacuum transfer holder

Software specifications

Acquisition Software:

  • JEOL TEM Centre
  • Gatan Digital Micrograph v3.62
  • JEOL SAAF Centre
  • JEOL Analysis Software

Supporting equipment

Sample Preparation:

  • IBSS Chiaro H2/N2 plasma cleaner
  • Henniker O2/Ar plasma cleaner
  • Melbuild LF4-CUBE pumping station

Data Analysis:

  • Offline analysis servers with Gatan Digital Micrograph > v3.34

Access rights

The EMU offers training, service, and collaboration for students, researchers, and industry professionals.

To begin using our facilities, please complete the enquiry form on the EMU website for general inquiries, training requests, or collaboration opportunities.

Acknowledgement

To acknowledge the use of this instrument in your publication, please copy and paste the following text into the acknowledgements section.

"This research used facilities funded by the Australian Research Council through LIEF grant (LE200100033), and supported by Microscopy Australia, including the scientific and technical assistance provided at the Electron Microscope Unit (EMU), within Mark Wainwright Analytical Centre (MWAC) at UNSW Sydney."

Instrument Type(s)

  • Aberration Corrected Transmission Electron Microscope

Manufacturer/Model

Owners

Dates

Identifiers

Funding